One-Step Simulated-Sunlight Adsorption-Photocatalytic Degradation of Diazinon and Triazophos Using a Corn-Stalk-Derived Hydrochar-Supported LDH/MOF Hybrid: Bicomponent Kinetics and Charge-Transfer Behavior

It includes dark adsorption experiments, photocatalyst-dose screening under LED, simulated sunlight, and UV-C irradiation, catalyst-free photolysis controls, pH and H₂O₂-dose experiments, concentration-dependent degradation profiles, kinetic-model calculations, and the 3 × 3 bicomponent DZN/TRZ concentration matrix.

Additional datasets include reactive-species scavenger experiments, electrochemical measurements of the individual materials and hybrid, post-use electrochemical characterization, real-water treatment experiments, COD measurements, Artemia salina acute toxicity results, catalyst reuse over eight consecutive cycles, and Mg, Fe, and Al leaching determined by ICP-OES. The files provide the numerical values used to generate the figures, statistical summaries, kinetic parameters, and comparative analyses reported in the associated manuscript, allowing verification and reuse of the experimental results.