Structure · dataset · 2018
CuO Rapid Synthesis with Different Morphologies by the Microwave Hydrothermal Method
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CuO structures were synthesized by microwave hydrothermal treatment using two different mineralizing agents (NaOH and NH4OH) and were evaluated as photocatalysts.
Description
The materials were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), and Brunauer-Emmett-Teller (BET) surface area analysis. The XRD patterns indicated the formation of the monoclinic phase in both samples with 13.78 and 14.23 nm crystallite size.
SEM analysis showed different agglomerates morphologies based on the mineralization agent employed. The CuO nanostructure synthesized with NH4OH presented agglomerated like-plates which results in a spherical shape, whereas the material synthesized with NaOH presented an agglomerate of larger plates. Both samples showed photocatalytic activity against RNL azo dye.
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The quasi-spherical shape CuO material reached 93 % of the discoloration.
Links
Where it is published
- Repository landing page scielo.figshare.com/articles/CuO_Rapid_Synthesis_with_Different_Morphologies_by_th… ↗
landing page · from DataCite
- DOI doi.org/10.6084/m9.figshare.7215848.v1 ↗
DOI / persistent id · from DataCite
Documentation and papers
- Creative Commons Attribution 4.0 International creativecommons.org/licenses/by/4.0/legalcode ↗
license · from DataCite
- IsSupplementTo 10.1590/1980-5373-mr-2018-0227 doi.org/10.1590/1980-5373-mr-2018-0227 ↗
publication · from DataCite
Catalogue records · 2
- DataCite API api.datacite.org/dois/10.6084/m9.figshare.7215848.v1 ↗
metadata API · from DataCite
- DataCite Commons commons.datacite.org/doi.org/10.6084/m9.figshare.7215848.v1 ↗
catalogue entry · from DataCite
Topics
- Stated by source
- Chemical engineering · Materials engineering
- Inferred from text
- Inorganic chemistry 71% · Microscopy 75%
Related
Provenance · 1 source records, 12 field assertions
| Source | Key | Last seen | Raw |
|---|---|---|---|
| DataCite | 10.6084/m9.figshare.7215848.v1 | 12 d ago | JSON v1 |
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|---|---|---|---|
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| byte_size | source · DataCite | connector:datacite@1.0.0 | |
| concepts[field].anzsrc:group:3402 | enrichment · DataCite | taxonomy-embedding@1.1.0 | title+keywords+description (71%) |
| concepts[field].fos:chemical-engineering | source · DataCite | connector:datacite@1.0.0 | |
| concepts[field].fos:materials-engineering | source · DataCite | connector:datacite@1.0.0 | |
| concepts[modality].local:modality:microscopy | enrichment · DataCite | keyword-concept-rules@1.0.0 | title+description (75%) |
| created_date | source · DataCite | connector:datacite@1.0.0 | |
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| publication_date | source · DataCite | connector:datacite@1.0.0 | /data/attributes/dates |
| title | source · DataCite | connector:datacite@1.0.0 | /data/attributes/titles/0/title |
| updated_date | source · DataCite | connector:datacite@1.0.0 |