← Search

Data · collection · 2016

β-(Methoxy-(substitutedphenyl)-methyl)-γ-butyrolactones: A short synthesis from cinnamyl acetate

Listed in DataCite

A simple and short synthesis has been revealed for the preparation of (±) β-(Methoxy-(substitutedphenyl)-methyl)-γ-butyrolactones.

Description

The reaction of cinnamyl acetate with Mn(OAc) 3 · 2H 2 O in boiling acetic acid containing acetic anhydride gave the products 2 and 3, which further cyclized in 3% H 2 SO 4 /CH 3 OH to afford the butyrolactones ( 8a–e ), which are intermediates of lignin, in good to moderate yields.

Links

Topics

From keywords
Ecology · Genetics · Microbiology
Provenance · 1 source records, 9 field assertions
SourceKeyLast seenRaw
DataCite10.6084/m9.figshare.c.217441415 d agoJSON v1
FieldAssertionExtractorEvidence
access_levelsource · DataCiteconnector:datacite@1.0.0/data/attributes/rightsList
concepts[field].fos:biological-sciencessource · DataCiteconnector:datacite@1.0.0
concepts[field].fos:health-sciencessource · DataCiteconnector:datacite@1.0.0
created_datesource · DataCiteconnector:datacite@1.0.0
descriptionsource · DataCiteconnector:datacite@1.0.0/data/attributes/descriptions
licensesource · DataCiteconnector:datacite@1.0.0/data/attributes/rightsList
publication_datesource · DataCiteconnector:datacite@1.0.0/data/attributes/dates
titlesource · DataCiteconnector:datacite@1.0.0/data/attributes/titles/0/title
updated_datesource · DataCiteconnector:datacite@1.0.0