Data and analysis scripts for: Large-Volume Low-Speed MAS NMR in High-Field Horizontal-Bore Systems Facilitated by 3D-Printing

Research data and analysis scripts supporting the manuscript "Large-Volume Low-Speed MAS NMR in High-Field Horizontal-Bore Systems Facilitated by 3D-Printing." The package contains the raw 79Br (KBr) and 1H MAS NMR datasets underlying the probe-head characterisation and the preliminary MAS demonstration, together with the Python scripts used to process them and generate the figures; and the rotor spinning-performance data from the parametric-optimisation studies (number of blades, blade angle, rotor-stator clearance, and wall thickness / sample volume), together with photographs of the 3D-printed rotor variants.

CAD models, STL files, slicer profiles and the tuning/matching PCB layouts are available from the authors on request.