Data · dataset · 2018
Fileset for "The role of residence time distribution in the continuous steady-state MSMPR crystallization of glycine"
Listed in DataCite
These are the supporting data files for the article "The role of residence time distribution in the continuous steady-state MSMPR crystallization of glycine".
Description
Abstract
In this work, a vacuum-driven intermittent transfer technique has been implemented to solve transfer line blockage issues and facilitate steady-state cooling crystallization studies of 𝛼-glycine in a single- and 2-stage MSMPR crystallizer. Experimental residence time distribution (RTD) analysis of the stirred tank MSMPR cascade is performed using an imperfect pulse method of the axial dispersion model to benchmark the mixing performance against that of tubular crystallizers and determine the influence of RTD on steady-state size distribution of 𝛼-glycine product.
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Process analytical technology (PAT) is used to monitor and understand crystallization process dynamics, and the effect of MSMPR operating temperature, mean residence time, and number of MSMPR stages on mean particle size, crystal size distribution, and yield is studied. Results show the significance of nucleation and growth mechanisms alongside RTD in determining steady-state size distribution, and the need for optimum control of supersaturation to benefit from improved RTDs provided by multistage MSMPR crystallizers.
Links
Where it is published
- Repository landing page repository.lboro.ac.uk/articles/Fileset_for_The_role_of_residence_time_distribution_i… ↗
landing page · from DataCite
- DOI doi.org/10.17028/rd.lboro.6429194 ↗
DOI / persistent id · from DataCite
Documentation and papers
- creativecommons.org /licenses/by-nc/4.0/legalcode ↗
Creative Commons Attribution Non Commercial 4.0 International
license · from DataCite
Catalogue records · 2
- DataCite API api.datacite.org/dois/10.17028/rd.lboro.6429194 ↗
metadata API · from DataCite
- DataCite Commons commons.datacite.org/doi.org/10.17028/rd.lboro.6429194 ↗
catalogue entry · from DataCite
Topics
- Stated by source
- Chemical engineering · Clinical medicine
- Inferred from text
- Chemical engineering 69%
Provenance · 1 source records, 11 field assertions
| Source | Key | Last seen | Raw |
|---|---|---|---|
| DataCite | 10.17028/rd.lboro.6429194 | 14 d ago | JSON v1 |
| Field | Assertion | Extractor | Evidence |
|---|---|---|---|
| access_level | source · DataCite | connector:datacite@1.0.0 | /data/attributes/rightsList |
| byte_size | source · DataCite | connector:datacite@1.0.0 | |
| concepts[field].anzsrc:group:4004 | enrichment · DataCite | taxonomy-embedding@1.1.0 | title+keywords+description (69%) |
| concepts[field].fos:chemical-engineering | source · DataCite | connector:datacite@1.0.0 | |
| concepts[field].fos:clinical-medicine | source · DataCite | connector:datacite@1.0.0 | |
| created_date | source · DataCite | connector:datacite@1.0.0 | |
| description | source · DataCite | connector:datacite@1.0.0 | /data/attributes/descriptions |
| license | source · DataCite | connector:datacite@1.0.0 | /data/attributes/rightsList |
| publication_date | source · DataCite | connector:datacite@1.0.0 | /data/attributes/dates |
| title | source · DataCite | connector:datacite@1.0.0 | /data/attributes/titles/0/title |
| updated_date | source · DataCite | connector:datacite@1.0.0 |