XRD, XPS, Raman and Excel data for the characterization of 3DPE and 3DPFE electrodes are presented in this paper

The data set includes Raman, GCD curve of 3DPE with different layers, capacity of 3DPE with different layers at different current densities, surface capacity of 3DPE with different layers at different current densities, surface capacity of 3DPE with different layers at the same current density, cycle curve of 3DPE-4, XPS C spectrum of GO and XPS of GA C spectrum, XPS of 3DPE-4 C spectrum, 3DPE and 3DPFE Raman, 3DPE and 3DPFE XRD, 3DPFE XPS S spectrum and Mo spectrum, CV of 3DPE-4 and 3DPFE-4, GCD of 3DPE-4 and 3DPFE-4, EIS of 3DPE-4 and 3DPFE-4, capacity contribution rate of 3DPFE.