Data · dataset · 2022
Data Set of Major Element of Red Sandstone Tafoni Samples in Danxiashan
Listed in ScienceDB
The major element analysis of 3 tafoni interior surface powder samples and 1 original sandstone powder sample was conducted on Agilent 720 inductively coupled plasma emission spectrometer (ICP-OES).
Description
During the experiment, about 0.05g of powder sample was placed in a PTFE container, and 0.6 ml HF and 3 ml HNO3 were added. Then the sealed container was placed in an electric furnace and heated to 185 ° C for about 36h.
After cooling, heat the container on the hot plate and allow it to evaporate to dryness, then add 200 ng Rh as the internal standard, then add 2 ml HNO3 and 4 ml water. Seal the container again and place it in an electric furnace at 135 ° C for about 5h to dissolve the residue. After cooling, it is measured by ICP-OES with dilution factor of 1000.
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The sample was digested by alkali fusion method to determine the content of silicon dioxide. Dissolve 0.05 g of sample in a silver crucible with 0.25 g NaOH at 700 ° C for about 30 min. After cooling, dissolve with hot water and acidify with 5 ml HCl, and finally add water to 250 ml for ICP-OES measurement.
About 1g sample is used for LOI. The sample is weighed in a porcelain crucible and heated in a muffle furnace at 900 ℃ for about 1 hour. The weight difference before and after ignition is LOI.
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Where it is published
- DOI doi.org/10.57760/sciencedb.06463 ↗
DOI / persistent id · from scidb cn
Catalogue records · 1
- OAI-PMH record scidb.cn/oai?verb=GetRecord&metadataPrefix=oai_dc&identifier=10.57760%2… ↗
metadata API · from scidb cn
Topics
- From keywords
- Earth & Environmental Science · Engineering · Humanities · Life Sciences · Social Science
Provenance · 1 source records, 10 field assertions
| Source | Key | Last seen | Raw |
|---|---|---|---|
| ScienceDB | 10.57760/sciencedb.06463 | 11 d ago | JSON v1 |
| Field | Assertion | Extractor | Evidence |
|---|---|---|---|
| access_level | source · scidb cn | connector:scidb_cn@1.0.0 | |
| concepts[field].local:field:earth-environmental | mapping · scidb cn | connector:scidb_cn@1.0.0 | |
| concepts[field].local:field:engineering | mapping · scidb cn | connector:scidb_cn@1.0.0 | |
| concepts[field].local:field:humanities | mapping · scidb cn | connector:scidb_cn@1.0.0 | |
| concepts[field].local:field:life-sciences | mapping · scidb cn | connector:scidb_cn@1.0.0 | |
| concepts[field].local:field:social-science | mapping · scidb cn | connector:scidb_cn@1.0.0 | |
| description | source · scidb cn | connector:scidb_cn@1.0.0 | /metadata/dc/description |
| license | source · scidb cn | connector:scidb_cn@1.0.0 | /metadata/dc/rights |
| publication_date | source · scidb cn | connector:scidb_cn@1.0.0 | |
| title | source · scidb cn | connector:scidb_cn@1.0.0 | /metadata/dc/title |