Data · dataset · 2022
In Situ Growth of Ultrathin Ni(OH)2 Nanosheets as Catalyst for Electrocatalytic Oxidation Reactions
Listed in ScienceDB
Figure 1.
Description
(a) SEM images, (b) TEM image (Inset: SAED pattern), (c) AFM image, (d) height profiles, (e) Ni2p spectrum, and (f) O1s spectrum of the as-synthesized Ni(OH)2/NF.Figure 2. (a) LSV curves of Ni(OH)2/NF and NF in 1.0 m KOH without and with 10 mm HMF.
(b) Tafel plots of Ni(OH)2/NF in 1.0 m KOH without and with 10 mm HMF (c) Cdl of Ni(OH)2/NF and NF in 1.0 m KOH (data derived from Figure S6). (d) Nyquist plots of Ni(OH)2/NF electrode in 1.0 m KOH without and with 10 mm HMF.Figure 3. (a) Chronoamperometric curves of Ni(OH)2/NF under different potentials in 1.0 m KOH solution containing 10 mm HMF.
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(b) Plot of HMF conversion and products yielded by Ni(OH)2/NF against reaction time in 1.0 m KOH solution containing 10 mm HMF at 1.39 V (vs. RHE). (c) Kinetic fitting curves for ECO of HMF to FDCA by Ni(OH)2/NF and NF. (d) Chronoamperometric curves and (e) FDCA yield and FE of Ni(OH)2/NF during five successive reuse cycles.
(f) SEM images of Ni(OH)2/NF after reuse cycles. (g, h) Ni2p and O1s XPS spectra of Ni(OH)2/NF before and after reuse cycles, and Ni(OH)2/NF (the spectra denoted as Activated) subjected to 1.39 V (vs. RHE) for 10 min.Figure 4. (a) Kinetic fitting plots of Ni(OH)2/NF from ECO of HMFCA and DFF to FDCA in 1.0 m KOH solution containing 5 mm of HMFCA or DFF at 1.39 V vs. RHE.
(b) Plots of reactant and product concentrations against reaction time for ECO of HMF catalyzed by Ni(OH)2/NF at 1.39 V (vs. RHE) potential in 25 mL 1.0 m KOH solution containing 50 mm HMF.Scheme 1. Reaction pathways for ECO of HMF to FDCA.
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Where it is published
- DOI doi.org/10.57760/sciencedb.06069 ↗
DOI / persistent id · from scidb cn
Catalogue records · 1
- OAI-PMH record scidb.cn/oai?verb=GetRecord&metadataPrefix=oai_dc&identifier=10.57760%2… ↗
metadata API · from scidb cn
Topics
- From keywords
- Earth & Environmental Science · Engineering · Humanities · Life Sciences · Social Science
- Inferred from text
- Image 75% · Nanotechnology 72%
Provenance · 1 source records, 11 field assertions
| Source | Key | Last seen | Raw |
|---|---|---|---|
| ScienceDB | 10.57760/sciencedb.06069 | 11 d ago | JSON v1 |
| Field | Assertion | Extractor | Evidence |
|---|---|---|---|
| concepts[field].anzsrc:group:4018 | enrichment · scidb cn | taxonomy-embedding@1.0.0 | title+keywords+description (72%) |
| concepts[field].local:field:earth-environmental | mapping · scidb cn | connector:scidb_cn@1.0.0 | |
| concepts[field].local:field:engineering | mapping · scidb cn | connector:scidb_cn@1.0.0 | |
| concepts[field].local:field:humanities | mapping · scidb cn | connector:scidb_cn@1.0.0 | |
| concepts[field].local:field:life-sciences | mapping · scidb cn | connector:scidb_cn@1.0.0 | |
| concepts[field].local:field:social-science | mapping · scidb cn | connector:scidb_cn@1.0.0 | |
| concepts[modality].local:modality:image | enrichment · scidb cn | keyword-concept-rules@1.0.0 | title+description (75%) |
| description | source · scidb cn | connector:scidb_cn@1.0.0 | /metadata/dc/description |
| license_text | source · scidb cn | connector:scidb_cn@1.0.0 | |
| publication_date | source · scidb cn | connector:scidb_cn@1.0.0 | |
| title | source · scidb cn | connector:scidb_cn@1.0.0 | /metadata/dc/title |