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Structure · dataset · 2026

Supplementary file 1_Protocol-dependent aging responses of polyurethane-bound pavement composites under thermo-oxidative, hygrothermal, and UV exposure.docx

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<p>Polyurethane-bound pavement composites offer high mechanical performance, but accelerated durability rankings can depend on how aging is imposed and which material response is measured.

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This study compared a moisture-curing methylene diphenyl diisocyanate-based polyether polyurethane binder and dense PC-13 composite under thermo-oxidative, hygrothermal, continuous ultraviolet (UV), intermittent UV, and intermittent UV–immersion exposure.

A 20 h thermo-oxidative group enabled duration-matched comparison with 20 h hygrothermal aging, and replicated mixture testing at 480 h supported Welch tests with Holm correction across the three UV protocols. At 20 h, thermo-oxidative aging reduced binder tensile strength to 13.52 MPa versus 18.13 MPa after hygrothermal aging and also produced lower elongation at break and splitting strength. Gel permeation chromatography and tetrahydrofuran-insoluble measurements showed that soluble-fraction molecular-mass changes did not reproduce the mechanical severity ranking.

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At 480 h, intermittent UV–immersion produced the lowest mean dynamic stability, flexural strain, and splitting strength, with retentions of 38.31%, 25.59%, and 52.57%, respectively. Flexural strain distinguished all three UV protocols, while the matched intermittent comparison showed a significant additional loss of dynamic stability when water immersion replaced 1 h of dark conditioning. Because continuous and intermittent schedules accumulated different UV-on times, those comparisons are interpreted only as whole-protocol contrasts.

The results demonstrate that durability assessment of polyurethane-bound pavement composites requires protocol-specific, multi-indicator interpretation.</p>

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NCL Dataoai:figshare.com:article/340692364 d agoJSON v1
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