Raw experimental dataset of structurally self-anchoring bipolar membranes with interlocked interfaces for coupled hydrogen production and biomass electrosynthesis

It contains raw characterization data including SEM, XPS and FTIR of the self-anchoring bipolar membranes with interlocked interfaces. Raw electrochemical data such as membrane impedance, ion transport and water dissociation voltage are included.

The dataset also covers hydrogen evolution performance, HPLC data of biomass electrooxidation products and long-term electrolysis stability data of the coupled electrolysis system. The designed structurally self-anchoring bipolar membrane with interlocked interface alleviates interfacial delamination and enables simultaneous hydrogen production at cathode and biomass electrosynthesis at anode. Raw test files and readme document are deposited for reproducing the structural and electrochemical results in this paper.